000117236 001__ 117236
000117236 005__ 20240319080955.0
000117236 0247_ $$2doi$$a10.3390/membranes12030266
000117236 0248_ $$2sideral$$a128641
000117236 037__ $$aART-2022-128641
000117236 041__ $$aeng
000117236 100__ $$aGarcía-Viñuales, S.
000117236 245__ $$aStudy of Melamine-Formaldehyde/Phase Change Material Microcapsules for the Preparation of Polymer Films by Extrusion
000117236 260__ $$c2022
000117236 5060_ $$aAccess copy available to the general public$$fUnrestricted
000117236 5203_ $$an-Eicosane-melamine formaldehyde microcapsules of an average size of 1.1 µm and latent heat of fusion of 146.2 ± 5.3 J/g have been prepared. They have been characterized by scanning electron microscopy, FTIR spectroscopy, calorimetric techniques, and thermogravimetric analyses. Under processing conditions, the microcapsules apparently preserved their properties, also maintaining their n-eicosane loading and heat storage capacity under washing conditions (water with detergent at 60¿C). The microcapsules synthesis has been scaled up for the fabrication of functional films by extrusion. For that, polymer films containing 10 wt.% of microcapsules were prepared at a pilot plant level. In those films, even though a fraction of the n-eicosane loading was lost during the extrusion process, the microcapsules showed good compatibility within the polyamide. The percentage of PCM in the polyamide 6 films was estimated by TGA, verifying also the heat storage capacity predicted by DSC (2.6 ± 0.7 J/g). © 2022 by the authors. Licensee MDPI, Basel, Switzerland.
000117236 536__ $$9info:eu-repo/grantAgreement/ES/MCIN/AEI/10.13039/501100011033$$9info:eu-repo/grantAgreement/ES/MINECO/RTC-2015-3503-5
000117236 540__ $$9info:eu-repo/semantics/openAccess$$aby$$uhttp://creativecommons.org/licenses/by/3.0/es/
000117236 590__ $$a4.2$$b2022
000117236 592__ $$a0.489$$b2022
000117236 591__ $$aCHEMISTRY, PHYSICAL$$b70 / 161 = 0.435$$c2022$$dQ2$$eT2
000117236 593__ $$aChemical Engineering (miscellaneous)$$c2022$$dQ2
000117236 591__ $$aPOLYMER SCIENCE$$b25 / 85 = 0.294$$c2022$$dQ2$$eT1
000117236 593__ $$aProcess Chemistry and Technology$$c2022$$dQ3
000117236 591__ $$aMATERIALS SCIENCE, MULTIDISCIPLINARY$$b137 / 343 = 0.399$$c2022$$dQ2$$eT2
000117236 593__ $$aFiltration and Separation$$c2022$$dQ3
000117236 591__ $$aENGINEERING, CHEMICAL$$b48 / 141 = 0.34$$c2022$$dQ2$$eT2
000117236 594__ $$a4.4$$b2022
000117236 655_4 $$ainfo:eu-repo/semantics/article$$vinfo:eu-repo/semantics/publishedVersion
000117236 700__ $$aRubio Hortells, C.
000117236 700__ $$0(orcid)0000-0002-0990-0422$$aMartínez-Izquierdo, L.$$uUniversidad de Zaragoza
000117236 700__ $$0(orcid)0000-0002-9934-1707$$aZornoza Encabo , B.$$uUniversidad de Zaragoza
000117236 700__ $$aPiera, E.
000117236 700__ $$aCaballero, M. Á.
000117236 700__ $$0(orcid)0000-0002-4954-1188$$aTéllez Ariso, C.$$uUniversidad de Zaragoza
000117236 7102_ $$15005$$2555$$aUniversidad de Zaragoza$$bDpto. Ing.Quím.Tecnol.Med.Amb.$$cÁrea Ingeniería Química
000117236 773__ $$g12, 3 (2022), 266 [13 pp]$$pMembranes$$tMembranes$$x2077-0375
000117236 8564_ $$s3447947$$uhttps://zaguan.unizar.es/record/117236/files/texto_completo.pdf$$yVersión publicada
000117236 8564_ $$s2745545$$uhttps://zaguan.unizar.es/record/117236/files/texto_completo.jpg?subformat=icon$$xicon$$yVersión publicada
000117236 909CO $$ooai:zaguan.unizar.es:117236$$particulos$$pdriver
000117236 951__ $$a2024-03-18-13:29:24
000117236 980__ $$aARTICLE