000126309 001__ 126309
000126309 005__ 20241125101153.0
000126309 0247_ $$2doi$$a10.1021/acsnano.3c00280
000126309 0248_ $$2sideral$$a133626
000126309 037__ $$aART-2023-133626
000126309 041__ $$aeng
000126309 100__ $$aQuirós-Ovies, R.$$uUniversidad de Zaragoza
000126309 245__ $$aMicrowave-driven exfoliation of bulk 2H-MoS[sub]2 after acetonitrile prewetting produces large-area ultrathin flakes with exceptionally high yield
000126309 260__ $$c2023
000126309 5060_ $$aAccess copy available to the general public$$fUnrestricted
000126309 5203_ $$a2D materials display exciting properties in numerous fields, but the development of applications is hindered by the low yields, high processing times, and impaired quality of current exfoliation methods. In this work we have used the excellent MW absorption properties of MoS2 to induce a fast heating that produces the near-instantaneous evaporation of an adsorbed, low boiling point solvent. The sudden evaporation creates an internal pressure that separates the MoS2 layers with high efficiency, and these are kept separated by the action of the dispersion solvent. Our fast method (90 s) gives high yields (47% at 0.2 mg/mL, 35% at 1 mg/mL) of highly exfoliated material (90% under 4 layers), large area (up to several μm2), and excellent quality (no significant MoO3 detected).
000126309 536__ $$9info:eu-repo/grantAgreement/EUR/ERC/ERC-AdG-742684$$9info:eu-repo/grantAgreement/EUR/ERC/ERC-PoC-842606$$9info:eu-repo/grantAgreement/ES/MINECO/CTQ2017-86060-P$$9info:eu-repo/grantAgreement/ES/MINECO/PID2020-116661RB-I00$$9info:eu-repo/grantAgreement/ES/MINECO/PID2021-127847OB-I00$$9info:eu-repo/grantAgreement/ES/MINECO/SEV-2016-0686
000126309 540__ $$9info:eu-repo/semantics/openAccess$$aby$$uhttp://creativecommons.org/licenses/by/3.0/es/
000126309 590__ $$a15.8$$b2023
000126309 592__ $$a4.593$$b2023
000126309 591__ $$aCHEMISTRY, PHYSICAL$$b14 / 178 = 0.079$$c2023$$dQ1$$eT1
000126309 593__ $$aEngineering (miscellaneous)$$c2023$$dQ1
000126309 591__ $$aNANOSCIENCE & NANOTECHNOLOGY$$b11 / 141 = 0.078$$c2023$$dQ1$$eT1
000126309 593__ $$aPhysics and Astronomy (miscellaneous)$$c2023$$dQ1
000126309 591__ $$aCHEMISTRY, MULTIDISCIPLINARY$$b15 / 231 = 0.065$$c2023$$dQ1$$eT1
000126309 593__ $$aNanoscience and Nanotechnology$$c2023$$dQ1
000126309 591__ $$aMATERIALS SCIENCE, MULTIDISCIPLINARY$$b27 / 439 = 0.062$$c2023$$dQ1$$eT1
000126309 593__ $$aMaterials Science (miscellaneous)$$c2023$$dQ1
000126309 594__ $$a26.0$$b2023
000126309 655_4 $$ainfo:eu-repo/semantics/article$$vinfo:eu-repo/semantics/publishedVersion
000126309 700__ $$aLaborda, M.
000126309 700__ $$aMartín Sabanés, N.
000126309 700__ $$aMartín-Pérez, L.
000126309 700__ $$aMoreno Da-Silva, S.
000126309 700__ $$aBurzurí, E.
000126309 700__ $$0(orcid)0000-0002-6873-5244$$aSebastian, V.$$uUniversidad de Zaragoza
000126309 700__ $$aPérez, E. M.
000126309 700__ $$0(orcid)0000-0002-8701-9745$$aSantamaría, J.$$uUniversidad de Zaragoza
000126309 7102_ $$15005$$2555$$aUniversidad de Zaragoza$$bDpto. Ing.Quím.Tecnol.Med.Amb.$$cÁrea Ingeniería Química
000126309 773__ $$g17, 6 (2023), 5984-5993$$pACS Nano$$tACS NANO$$x1936-0851
000126309 8564_ $$s8408147$$uhttps://zaguan.unizar.es/record/126309/files/texto_completo.pdf$$yVersión publicada
000126309 8564_ $$s3139705$$uhttps://zaguan.unizar.es/record/126309/files/texto_completo.jpg?subformat=icon$$xicon$$yVersión publicada
000126309 909CO $$ooai:zaguan.unizar.es:126309$$particulos$$pdriver
000126309 951__ $$a2024-11-22-12:07:44
000126309 980__ $$aARTICLE