doi:10.1039/c4ra16284fengNavarro, MartaMateo, EsterDiosdado, BeatrizTsapatsis, MichaelCoronas, JoaquínActivation of giant silicalite-1 monocrystals combining rapid thermal processing and ozone calcinationART-2015-89323A rapid thermal processing (RTP) technique combined with ozone/oxygen calcination was applied to activate and heal the structure of a 1.1 mm2 section of a silicalite-1 giant monocrystal. Crystallinity was monitored by single crystal X-ray diffraction and high sensitive thermogravimetry (TGA) was performed to prove the complete removal of the structure directing agent.2015http://zaguan.unizar.es/record/6993910.1039/c4ra16284fhttp://zaguan.unizar.es/record/69939oai:zaguan.unizar.es:69939info:eu-repo/grantAgreement/ES/MINECO/MAT2010-15870RSC Advances 5, 23 (2015), 18035-18040by-nchttp://creativecommons.org/licenses/by-nc/3.0/es/info:eu-repo/semantics/openAccess