Resumen: In this study, an example of the reuse and revalorization of lignocellulosic waste from carnauba palm (Copernicia prunifera) leaves, macauba palm (Acrocomia aculeata) endocarp (shell) and European stone pine (Pinus pinea) nut shell is presented for the first time. The physical-chemical adsorption of Rhodamine B (RhB) dye for the different materials is studied in detail, together with the thermodynamic feasibility and the spontaneous and endothermic nature of the biosorption process. Subsequently, the production of total reducing sugars (TRS) is compared by enzymatic hydrolysis (before and after the adsorption process of the RhB pollutant), confirming the viability of TRS production in all cases, with yields ranging from 65.9% for pine nut shell (after adsorption) to 74.9% for the carnauba endocarp and to 84.0% for carnauba leaves (before adsorption). Hence the use of lignocellulosic materials as adsorbents does not preclude their ulterior reuse for obtaining fermentable sugars by enzymatic hydrolysis. Idioma: Inglés Año: 2017 Publicado en: CELLULOSE CHEMISTRY AND TECHNOLOGY 51, 1-2 (2017), 127-136 ISSN: 0576-9787 Originalmente disponible en: Texto completo de la revista