Activation of giant silicalite-1 monocrystals combining rapid thermal processing and ozone calcination

Navarro, Marta ; Mateo, Ester (Universidad de Zaragoza) ; Diosdado, Beatriz (Universidad de Zaragoza) ; Tsapatsis, Michael ; Coronas, Joaquín (Universidad de Zaragoza)

Resumen: A rapid thermal processing (RTP) technique combined with ozone/oxygen calcination was applied to activate and heal the structure of a 1.1 mm2 section of a silicalite-1 giant monocrystal. Crystallinity was monitored by single crystal X-ray diffraction and high sensitive thermogravimetry (TGA) was performed to prove the complete removal of the structure directing agent.

Idioma: Inglés

DOI: 10.1039/c4ra16284f

Año: 2015

Publicado en: RSC Advances 5, 23 (2015), 18035-18040
ISSN: 2046-2069

Factor impacto JCR: 3.289 (2015)

Categ. JCR: CHEMISTRY, MULTIDISCIPLINARY rank: 48 / 163 = 0.294 (2015) - Q2 - T1

Factor impacto SCIMAGO: 0.947 - Chemistry (miscellaneous) (Q1) - Chemical Engineering (miscellaneous) (Q1)

Financiación: info:eu-repo/grantAgreement/ES/MINECO/MAT2010-15870

Tipo y forma: Article (Published version)

Área (Departamento): Área Ingeniería Química (Dpto. Ing.Quím.Tecnol.Med.Amb.)
Área (Departamento): Área Didáctica Ciencias Exper. (Dpto. Didáctica Cienc. Experi.)
Área (Departamento): Servicios. Div.Caract.Físi.Quí (Serv.Gral. Apoyo Investigación)