Resumen: A rapid thermal processing (RTP) technique combined with ozone/oxygen calcination was applied to activate and heal the structure of a 1.1 mm2 section of a silicalite-1 giant monocrystal. Crystallinity was monitored by single crystal X-ray diffraction and high sensitive thermogravimetry (TGA) was performed to prove the complete removal of the structure directing agent. Idioma: Inglés DOI: 10.1039/c4ra16284f Año: 2015 Publicado en: RSC Advances 5, 23 (2015), 18035-18040 ISSN: 2046-2069 Factor impacto JCR: 3.289 (2015) Categ. JCR: CHEMISTRY, MULTIDISCIPLINARY rank: 48 / 163 = 0.294 (2015) - Q2 - T1 Factor impacto SCIMAGO: 0.947 - Chemistry (miscellaneous) (Q1) - Chemical Engineering (miscellaneous) (Q1)